Synthesis of multicomponent nanocomposites containing filamentary carbon nanostructures / R. V. Sazonov, G. E. Kholodnaya, D. V. Ponomarev [et al.]

Set Level: Fullerenes, Nanotubes and Carbon NanostructuresCoauthor: Sazonov, R. V., physicist, senior researcher of Tomsk Polytechnic University, candidate of physico-mathematical Sciences, 1984-, Roman Vladimirovich;Kholodnaya, G. E., electrophysicist, Associate Scientist of Tomsk Polytechnic University, candidate of technical Sciences, 1986-, Galina Evgenievna;Ponomarev, D. V., physicist, Senior researcher of Tomsk Polytechnic University, Candidate of technical sciences, 1981-, Denis Vladimirovich;Sivkov, A. A., Specialist in the field of electric power engineering, Professor of Tomsk Polytechnic University, Doctor of technical sciences, 1951-, Aleksandr Anatolyevich;Shanenkov, I. I., specialist in the field of electric power engineering, Associate Professor of the Department of Tomsk Polytechnic University, Candidate of Sciences, 1990-, Ivan Igorevich;Zhirkov, I. S., Igor SergeevichCorporate Author (Secondary): Национальный исследовательский Томский политехнический университет, Исследовательская школа физики высокоэнергетических процессов, (2017- );Национальный исследовательский Томский политехнический университет, Инженерная школа новых производственных технологий, Научно-производственная лаборатория "Импульсно-пучковых, электроразрядных и плазменных технологий";Национальный исследовательский Томский политехнический университет, Инженерная школа энергетики, Отделение электроэнергетики и электротехники (ОЭЭ)Language: английский.Country: Великобритания.Abstract: In this work, the multicomponent nanocomposites containing filamentary carbon nanostructures were synthesized using materials based on iron oxides with a predominant content of the epsilon phase (e-Fe2O3). These iron oxide-based materials were obtained by a direct plasma-dynamic synthesis with supersonic outflow of an iron-containing electric discharge plasma into an oxygen atmosphere. Subsequently, they were used as an initial precursor and placed in the plasma-chemical reactor, where the multicomponent C/SixOy/Fe2O3 nanostructures were synthesized under the influence of the pulsed electron beam. This method was based on the volume excitation of the reaction gas by a pulsed electron beam in such a way as to control the uniform process implementation in the entire excitation region. The morphology and phase composition of the synthesized C/SixOy/Fe2O3 nanocomposites were studied. A typical morphological feature of the C/SixOy/Fe2O3 samples was found to be the formation of filamentary nanostructures. Their diameter does not exceed 10–20 nm, while their length varies up to 1 µm..Bibliography: [References: 29 tit.].Audience: .Subject: электронный ресурс | труды учёных ТПУ | plasma dynamic synthesis | plasma chemical synthesis | pulsed electron beam | composite | silicon oxide | carbon structures | iron oxide | плазмохимический синтез | композиты | оксид кремния | углеродные структуры | плазмодинамический синтез | электронные пучки Online Resources:Click here to access online
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[References: 29 tit.]

In this work, the multicomponent nanocomposites containing filamentary carbon nanostructures were synthesized using materials based on iron oxides with a predominant content of the epsilon phase (e-Fe2O3). These iron oxide-based materials were obtained by a direct plasma-dynamic synthesis with supersonic outflow of an iron-containing electric discharge plasma into an oxygen atmosphere. Subsequently, they were used as an initial precursor and placed in the plasma-chemical reactor, where the multicomponent C/SixOy/Fe2O3 nanostructures were synthesized under the influence of the pulsed electron beam. This method was based on the volume excitation of the reaction gas by a pulsed electron beam in such a way as to control the uniform process implementation in the entire excitation region. The morphology and phase composition of the synthesized C/SixOy/Fe2O3 nanocomposites were studied. A typical morphological feature of the C/SixOy/Fe2O3 samples was found to be the formation of filamentary nanostructures. Their diameter does not exceed 10–20 nm, while their length varies up to 1 µm.

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