Arenediazonium Tosylates (ADTs) as Efficient Reagents for Suzuki–Miyaura Cross-Coupling in Neat Water / K. V. Kutonova [et al.]

Set Level: Synthesis, international full-paper journal = 1969-Coauthor: Kutonova, K. V., chemist, Engineer of Tomsk Polytechnic University, 1990-, Ksenia Valentinovna;Jung, N., Nicole;Trusova, M. E., organic chemist, Associate professor of Tomsk Polytechnic University, Candidate of chemical sciences, 1982-, Marina Evgenievna;Filimonov, V. D., Russian chemist, Professor of the TPU, 1945-, Viktor Dmitrievich;Postnikov, P. S., organic chemist, Associate Professor of Tomsk Polytechnic University, Candidate of chemical sciences, 1984-, Pavel Sergeevich;Brase, S., StefanCorporate Author (Secondary): Национальный исследовательский Томский политехнический университет (ТПУ), Институт физики высоких технологий (ИФВТ), Кафедра биотехнологии и органической химии (БИОХ);Национальный исследовательский Томский политехнический университет (ТПУ), Институт природных ресурсов (ИПР), Кафедра технологии органических веществ и полимерных материалов (ТОВПМ)Language: английский.Country: Россия.Abstract: A simple, convenient, and environment-friendly procedure for the preparation of substituted biaryls via Suzuki–Miyaura cross-coupling­ was developed. The use of arenediazonium tosylates and corresponding boron compounds allows a conversion in neat water in the presence of commercially available Pd(OAc)2 under mild conditions with tolerance to a wide range of functional groups. A procedure particularly useful for the synthesis of di-ortho-substituted biaryls was developed..Bibliography: [References: p. 1687-1688 (23 tit.)].Audience: .Subject: электронный ресурс | труды учёных ТПУ | реакции Сузуки-Мияуры | водные среды | бифенилы | тозилатные соли арилдиазония Online Resources:Click here to access online
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[References: p. 1687-1688 (23 tit.)]

A simple, convenient, and environment-friendly procedure for the preparation of substituted biaryls via Suzuki–Miyaura cross-coupling­ was developed. The use of arenediazonium tosylates and corresponding boron compounds allows a conversion in neat water in the presence of commercially available Pd(OAc)2 under mild conditions with tolerance to a wide range of functional groups. A procedure particularly useful for the synthesis of di-ortho-substituted biaryls was developed.

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